In terms of organic molecules, the work is divided into formation of carbon-carbon bonds, introduction of heteroatoms and heteroatom interconversions. Thus, Volumes focus on carbon-carbon formation, but also include aspects of heteroatom introduction. Volumes concentrate on interconversion of heteroatoms, but also deal with exchange of carbon-carbon bonds for carbon-heteroatom bonds.
Formation of Nitriles, Carboxylic Acids, and Derivatives by Oxidation, Substitution, and Addition
Organization of the chapters is along the theme of selectivity, which is a critical question in determining the suitability of a synthetic method. Volume 9 contains cumulative author and subject indexes. Page Count: Print - Hardcover Delivery may take up to 10 days.
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Comprehensive Organic Synthesis Oxidation
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Institutional Subscription. Free Shipping Free global shipping No minimum order. Group 3 Glossary 8. Ludwig-Maximilians-Universitat, Munich, Germany. University of Pennsylvania, USA. Powered by. You are connected as. In this article we would like to report a simple and convenient method for the effective conversion of alcohols to their corresponding aldehydes or ketones under heterogeneous conditions.
The striking features of our method are: short reaction times, formation of no over oxidation products due to high selectivity and mild nature of oxidant, easy work-up procedure, high yields and carbon carbon double or triple bond functional group in the alcohol structure does not oxidize to other functional group. Scheme 5 shows the proposed mechanism for this oxidation. Thallium nitrate TTN.
Moffatt‐Swern Oxidation - - Major Reference Works - Wiley Online Library
The excess solvent was evaporated under reduced pressure using a rotary evaporator. The white powder solid was dried in vacuum desiccators.
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General procedure for oxidation of alcohols in solution. In a round-bottomed flask 25 mL equipped with a magnetic stirrer and condenser, a solution of alcohols 1 mmol and DMSO 0. After completion, the reaction mixture was filtrate and the solid material was washed with CH 3 CN 10 mL.
The filtrate was evaporated and the resulting crude material was purified by column chromatography on silica gel to afford the pure product.
Products were characterized by their physical constants, comparison with authentic samples and IR and NMR spectra. Trost, I.tranguijerkcamtaitel.tk
Comprehensive Organic Synthesis - Volume 4 (1991)
Fleming, S. Tojo, M. Lorber, J. Osborn, Tetrahedron Lett. Hosseini-Monfared, C. Nather, H.
Winkler, C. Janiak, Inorganica Chimica Acta , 75, Rajabi, B.
Karimi, J. A: Chem. Sheldon, I. Arends, A. Dijkman, Catal.
Today, 57 , Taylor, C. Chiang, A.
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